CH437 and CH637
Spectroscopic Techniques in Organic Chemistry
S. C. Blackstock, Fall 2005, Department of Chemistry, The University of Alabama, Tuscaloosa, AL
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Announcements


exam 3 update due 12-6
assignment: Pavia 10.9,
tripeptide
due 12-8

answers to assigned problems

exam 3 - Dec. 1 @ 7:30 AM

10.2,10.8,9.37, C13H20O - due 11-22
graduate student assignment

exam 2 - Nov. 1 @ 7PM

exam 2 F04 key posted
ch6 hmwk returned on 11-1

ch6: 7-8, 11, 14-20 - due 10-27

ch4: 12-16, Smith 6, 54 - due 10-20

ch4: 7-11, SCB#2#,3 - due 10-18

Announcement archive
2005 Exams

exam 1   key

exam 2  key

exam3 questions, exam 3 spectra

final exam

 

 

lecture outlines

handouts and problems

syllabus

JOC author info-cmpd characterization, spectroscopy references

Chapter 1 lecture outline
Molecular Formula Determination

#8, #11, #15

Chapter 2 lecture outline
IR Spectroscopy

IR stretches , IR table, #25, #55, #75, #76, #9.4, #9.5, problem set #1

Chapter 3 lecture outline
1H NMR spectroscopy (basics)

atom magnetic properties, 1H-NMR shifts , CM-table, 1H-J table, d-solvent NMR properties, H2O in d-solvents, organic solvent NMR data, #9.35, 4.3a-i, problem set #2, Fig 3.16, Fig 3.20, Fig 3.5/3.6

Chapter 4 lecture outline
13C-, 19F-, 31P-NMR Spectroscopy

13C-NMR shifts

Chapter 5 lecture outline
1H NMR Spectroscopy (spin coupling)

SCB #1, SCB#2, SCB#3, #5.13, ipsenol, stereochem,

Chapter 6 lecture outline
Advanced Topics in 1-D NMR


Chapter 7 lecture outline
UV-vis Spectroscopy


Chapter 8 lecture outline
Mass Spectrometry


Chapter 10 lecture outline
Advanced 2D NMR Techniques


old exams and quizzes (2003 and 2004)

exam1_F04.pdf    key

exam 1 (2003, KHS)     key

exam2_F04.pdf    key

exam 2 (2003, KHS)     key

exam3_F04.pdf    key

final part 1 (2003, KHS)   part 2 (2003, KHS)

 

  

final exam F04.pdf   key

quiz 1 (2003, KHS)   key        quiz 3 (2003, KHS)   key

 

quiz 2 (2003, KHS)   key        quiz 4 (2003, KHS)   key

LINKS:

Merlic Webspectra (UCLA)
Smith Spectral Problems (Notre Dame)
Integrated Spectral Database System (SDBS)